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The total yield of pure methyl red is 790—840 g.

When the methyl red is crystallized from toluene, it sometimes separates in the form of bright-red lumps, probably on account of too rapid crystallization.

In the meantime a second conical flask containing 1250 cc. of toluene is attached to the funnel, and a new charge of 150 g. of crude methyl red is placed in the paper.

The crystals of methyl red are filtered off and washed with a little toluene.

The watery mother liquors from the crude methyl red are rendered alkaline with sodium hydroxide and distilled until no more dimethylaniline passes over.